Transition Metals & Complex Ions

20min Part 3 / Ch6 / Lesson 3
Prerequisites: 3-6-1 , 3-6-2

Objectives

  • Describe the characteristics of transition metals
  • Know the names and colors of common complex ions
  • Understand the systematic separation of metal ions

Characteristics of Transition Metals

Transition metals (Groups 3–11) share common features:

  • Variable oxidation states (Fe²⁺/Fe³⁺, Cu⁺/Cu²⁺, etc.)
  • Colored compounds are common
  • Many serve as catalysts (Fe, Pt, V₂O₅, MnO₂, etc.)
  • Form complex ions readily

Iron Compounds

PropertyFe²⁺ (iron(II))Fe³⁺ (iron(III))
Solution colorPale greenYellow-brown
HydroxideFe(OH)₂ (green-white)Fe(OH)₃ (red-brown)
With KSCNNo changeBlood-red
With K₄[Fe(CN)₆]Dark blue precipitate (Turnbull’s blue)Dark blue precipitate
With K₃[Fe(CN)₆]Dark blue precipitateNo change (brown)

Comparing Fe²⁺ and Fe³⁺

Copper Compounds

CompoundColorNotes
CuSO₄ (anhydrous)WhiteUsed to detect water
CuSO₄·5H₂OBlueBlue vitriol
Cu(OH)₂Blue-whiteHeated → CuO (black)
CuOBlackCopper(II) oxide
Cu₂ORedFormed in Fehling’s test

Complex Ions

Complex ions: metal ions bonded to ligands via coordinate bonds.

Key examples:

Complex ionColorFormation
[Cu(NH₃)₄]²⁺Deep blueCu²⁺ + excess NH₃
[Ag(NH₃)₂]⁺ColorlessAg⁺ + NH₃ → AgCl dissolves
[Zn(OH)₄]²⁻ColorlessZn²⁺ + excess NaOH
[Al(OH)₄]⁻ColorlessAl³⁺ + excess NaOH
[Fe(CN)₆]⁴⁻YellowFe²⁺ + CN⁻

Systematic Separation of Metal Ions

Mixed solution (Ag⁺, Pb²⁺, Cu²⁺, Fe³⁺, Al³⁺, Zn²⁺, Na⁺…)+ HClPrecipitate: AgCl↓, PbCl₂↓+ H₂S (acidic)Precipitate: CuS↓, PbS↓ (black)+ NH₃ + H₂SPrecipitate: Fe(OH)₃↓, Al(OH)₃↓+ H₂S (basic)Precipitate: ZnS↓ (white)Remaining: Na⁺, K⁺ → flame test
Systematic separation of metal ions

Check Your Understanding

Q1 What color forms when KSCN is added to Fe³⁺ solution?

Q2 What happens when excess NH₃ is added to Cu²⁺?

Q3 What color is anhydrous CuSO₄?


Exercises

Q1. Describe how to separate Ag⁺, Cu²⁺, and Fe³⁺ from a mixed solution.

Solution
  1. Add HCl → AgCl (white) precipitates. Filter to separate Ag⁺.
  2. To the filtrate, pass H₂S (acidic conditions) → CuS (black) precipitates. Filter to separate Cu²⁺.
  3. Boil to remove H₂S, then add NaOH → Fe(OH)₃ (red-brown) precipitates. Fe³⁺ is separated.